14774-37-9, Tetrahydropyran-4-methanol is a Tetrahydropyrans compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
To a solution of tetrahydropyran-4-methanol (5.0 g, 43 mmol) in dichlormethane (30 mL) was added triethylamine (7.2 mL, 51.6 mmol). The mixture was cooled to 0 C., and methane sulfonyl chloride (4.0 mL, 51.6 mmol) was added. The mixture was stirred in an ice bath for several hours and was slowly warmed to RT. The reaction then was stirred at RT for 18 h. The reaction was concentrated in vacuo. The residue was taken up in EtOAc and was washed with saturated NaHCO3. The organic layer was dried [MgSO4], filtered, and concentrated in vacuo to give the mesylate Part A(v)(a) compound (8.3 g, quantitative yield) as a white, needle-like solid.
14774-37-9, 14774-37-9 Tetrahydropyran-4-methanol 2773573, aTetrahydropyrans compound, is more and more widely used in various.
Reference£º
Patent; Bristol-Myers Squibb Company; US2008/21052; (2008); A1;,
Tetrahydropyran – Wikipedia
Tetrahydropyran – an overview | ScienceDirect Topics