Extracurricular laboratory: Synthetic route of 50501-07-0

When you point to this article, it is believed that you are also very interested in this compound(50501-07-0)Quality Control of Ethyl indoline-2-carboxylate and due to space limitations, I can only present the most important information.

In organic chemistry, atoms other than carbon and hydrogen are generally referred to as heteroatoms. The most common heteroatoms are nitrogen, oxygen and sulfur. Now I present to you an article called Introduction of heterocycles at the 2-position of indoline as ester bioisosteres, published in 2004-02-20, which mentions a compound: 50501-07-0, mainly applied to indoline heterocyclic derivative preparation cyclization, Quality Control of Ethyl indoline-2-carboxylate.

Compounds were prepared with heterocyclic replacements for metabolically unstable esters of benzopyranyl indole-2-carboxylic esters, which showed good in vitro and in vivo cardioprotective efficacies possibly through the opening of mitochondrial ATP-sensitive potassium channel (KATP). Initially, indolin-2-yl-heterocycles were constructed using unprotected indoline-2-carboxylic acid, but the cyclization was proceeded with oxidation of the indoline ring to the indole, which did not react with benzopyranyl epoxide. An N-BOC group was introduced to deplete the electron d. of the indoline ring. Various indolin-2-yl-heterocycles, such as I and II, were prepared by the cyclization of the building blocks including carboxamide, β-hydroxy amide, hydrazide, nitrile starting from N-BOC-indoline-2-carboxylic acid.

When you point to this article, it is believed that you are also very interested in this compound(50501-07-0)Quality Control of Ethyl indoline-2-carboxylate and due to space limitations, I can only present the most important information.

Reference:
Tetrahydropyran – Wikipedia,
Tetrahydropyran – an overview | ScienceDirect Topics