Analyzing the synthesis route of 14774-37-9

As the paragraph descriping shows that 14774-37-9 is playing an increasingly important role.

With the rapid development and complex challenges of chemical substances, new drug synthesis pathways are usually the most effective.14774-37-9,Tetrahydropyran-4-methanol,as a common compound, the synthetic route is as follows.

Pyridinium chlorochromate (445mg,)Add to the reaction flask and dissolve with 5 mL of dichloromethane.45 (200 mg,) was slowly added dropwise to a solution of pyridinium chlorochromate in dichloromethane.The reaction was carried out for 1.5 h at room temperature, and the reaction was completely detected by TLC, and filtered with celite.Column chromatography (PE: EA = 5:1) gave a colorless, transparent liquid, 124 mg, yield 63%., 14774-37-9

As the paragraph descriping shows that 14774-37-9 is playing an increasingly important role.

Reference£º
Patent; Xihua University; Qian Shan; Li Guobo; Chen Yang; Li Chao; Zhang Man; Wang Zhouyu; Yang Lingling; Lai Peng; (16 pag.)CN108689938; (2018); A;,
Tetrahydropyran – Wikipedia
Tetrahydropyran – an overview | ScienceDirect Topics