36838-71-8, 4-Methylenetetrahydro-2H-pyran is a Tetrahydropyrans compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
General procedure: In a dry two-neck round-bottom flask equipped with a condenser and a magnetic stirrer were successively added oxime1b(1 or 2 eq., See Table 2), iodoester8(1 eq.) and the desired alkene partner (4-5 eq.) in benzene (0.4 M). Argon was then bubbled directly into the flask for 30 min. (Bu3Sn)2(1.5 eq.) was then injected and the flask was heated to 60C. DTBHN was added after 5min., then every 90 min if required (TLC). After total consumption of the starting iodide, the resulting mixture was concentrated in vacuo and purified by silica gel chromatography (Petroleum ether/EtOAc) to afford the desired product., 36838-71-8
The synthetic route of 36838-71-8 has been constantly updated, and we look forward to future research findings.
Reference£º
Article; Landais, Yannick; Robert, Frederic; Godineau, Edouard; Huet, Laurent; Likhite, Nachiket; Tetrahedron; vol. 69; 47; (2013); p. 10073 – 10080;,
Tetrahydropyran – Wikipedia
Tetrahydropyran – an overview | ScienceDirect Topics