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Molecular and spectroscopic properties of chloride and thiocyanate hydridecarbonyl ruthenium(II) complexes with pyridine derivative ligands

[RuH(CO)(dpa)(PPh3)2]X and [RuHX(CO)(pyCHPh)(PPh 3)2] (X = Cl, NCS) complexes (where dpa = 2,2?-dipyridylamine, pyCHPh = 4-(3-phenylpropyl)pyridine) have been prepared and studied using IR, NMR, UV-Vis spectroscopies and X-ray crystallography. The electronic structures and bonding of the obtained complexes were defined on the basis of the DFT method. The electronic spectra of the complexes were calculated and associated with the structure of the molecular orbitals of the complexes. The luminescence properties of the complexes were determined.

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Tetrahydropyran – Wikipedia,
Tetrahydropyran – an overview | ScienceDirect Topics

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Monomers, Oligomeric Complexes, Coordination Polymers, and Methods for Their Preparation and Use

Implementations and techniques for preparing and using monomers, oligomeric complexes, and coordination polymers are generally disclosed.

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Tetrahydropyran – Wikipedia,
Tetrahydropyran – an overview | ScienceDirect Topics

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A catalyst don’t appear in the overall stoichiometry of the reaction it catalyzes, but it must appear in at least one of the elementary reactions in the mechanism for the catalyzed reaction. 499-40-1, Name is (2R,3S,4R,5R)-2,3,4,5-Tetrahydroxy-6-(((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl)oxy)hexanal, molecular formula is C12H22O11. In a Article£¬once mentioned of 499-40-1, Safety of (2R,3S,4R,5R)-2,3,4,5-Tetrahydroxy-6-(((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl)oxy)hexanal

An unique trinuclear triply bridged Cu(II) compound containing double acetato and single azido bridges: Synthesis, X-ray structure and magnetism of [Cu3(dpyam)2(mu1,1-N3) 2(mu-CH3COO- kappa-O1)2(mu-CH3COO-kappa-O 1,O2)2]

The synthesis, characterization, crystal structure and magnetic properties of the unique azido-acetato bridged trinuclear triply bridged Cu(II) compound, [Cu3(dpyam)2(mu1,1-N3) 2(mu-CH3COO-kappa-O1)2(mu- CH3COO-kappa-O1,O2)2] ¡¤ 2(H2O), is reported. In the centrosymmetric compound, the central Cu atom is linked to two terminal Cu atoms by a double acetato bridge and an azido bridge, thereby providing a linear trinuclear unit. The coordination geometry around each of the terminal Cu(II) ions is distorted square pyramidal, while the geometry of the central Cu(II) ion is elongated octahedral. The magnetic susceptibility measurements, measured from 5 to 300 K revealed a weak antiferromagnetic interaction between the Cu(II) ions with a J value of -10.2 cm-1. In the EPR no signals for the low-lying doublet are resolved at 77 K.

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Tetrahydropyran – Wikipedia,
Tetrahydropyran – an overview | ScienceDirect Topics

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New Luminescent Polynuclear Metal Complexes with Anticancer Properties: Toward Structure-Activity Relationships

A series of new heterodinuclear luminescent complexes with two different organic ligands have been synthesized and characterized. A luminescent RuII(polypyridine) moiety and a metal-based anticancer fragment (AuCl, (p-cymene)RuCl2, (p-cymene)OsCl2, (Cp?)RhCl2, or Au-thioglucose) are the two general features of these complexes. All of the bimetallic compounds have been evaluated for their antiproliferative properties in vitro in human cancer cell lines. Only the complexes containing an Au(I) fragment exhibit antiproliferative activity in the range of cisplatin or higher. The photophysical and electrochemical properties of the bimetallic species have been investigated, and fluorescence microscopy experiments have been performed successfully. The most promising bimetallic cytotoxic complexes (i.e., with the Au-thioglucose scaffold) have shown to be easily taken up by cancer cells at 37 C in the cytoplasm or in specific organelles. Interestingly, experiments repeated at 4 C showed no uptake of the bimetallic species inside cells, which confirms involvement of active transport processes. To evaluate the role of glucose transporters in the cell uptake of the gold complexes, inhibition of the GluT-1 (glucose transporter isoform with high level of expression in cancer cells) was achieved, showing only scarce influence on the compounds’ uptake. Finally, the observed absence of interactions with nucleic acid model structures suggests that the gold compounds may have different intracellular targets with respect to cisplatin.

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Tetrahydropyran – Wikipedia,
Tetrahydropyran – an overview | ScienceDirect Topics

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Nickel-diflunisal complexes: Synthesis, characterization, in vitro antioxidant activity and interaction with DNA and albumins

The reaction of NiCl2 with the non-steroidal anti-inflammatory drug diflunisal (Hdifl) resulted in the formation of complex [Ni(difl-O)2(MeOH)4], 1. The co-existence of a N,N’-donor heterocyclic ligand 2,2?-dipyridylketone oxime (Hpko), 1,10-phenanthroline (phen), 2,2?-bipyridine (bipy) and 2,2?-bipyridylamine (bipyam) led to the formation of complexes [Ni(difl-O)2(Hpko-N,N’)2], 2, [Ni(difl)2(phen)(MeOH)2], 3, [Ni(difl)2(bipy)(MeOH)2], 4 and [Ni(difl-O,O’)2(bipyam)], 5, respectively. The complexes were characterized by physicochemical and spectroscopic techniques and the crystal structures of complexes 1 and 2 were determined by X-ray crystallography. The ability of the complexes to scavenge in vitro 1,1-diphenyl-picrylhydrazyl, 2,2?-azinobis(3-ethylbenzothiazoline-6-sulfonic acid) and hydroxyl radicals was investigated; the complexes were more active scavengers than free Hdifl. The interaction of the complexes with serum albumins was investigated by fluorescence emission spectroscopy and the binding constants of the compounds to the albumins were calculated. UV spectroscopy, cyclic voltammetry and viscosity measurements as well as fluorescence emission spectroscopy for the competitive studies of the complexes with ethidium bromide were employed so as to monitor the interaction of the compounds with calf-thymus DNA and revealed intercalation as the most possible mode of binding.

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Tetrahydropyran – Wikipedia,
Tetrahydropyran – an overview | ScienceDirect Topics

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Dinuclear copper(II) phosphonates containing chelating nitrogen ligands: Synthesis, structure, magnetism and nuclease activity

The reaction of Cu(ClO4)2¡¤6H2O with RPO 3H2 (R = cyclopen-tyl, isopropyl, trichloromethyl) in the presence of chelating nitrogen ligands bpya or bpy afforded dinuclear copper phosphonates. [Cu2 (mu2-C5H 9PO3) 2 (bpya) 2 (H2O) 2] (H2O) 4 (1) [Cu2 (mu2-C3H7PO3) 2 (bpya) 2 (H2O) 2] (H2O) 2 (2) and [Cu2 (mu2-CCl3PO3) 2 (bpy) 2 (MeOH) 2] (H2O) (3) [bpya = 2, 2′-bipyridyl-amine, bpy = 2, 2′-bipyridine]. The molecular structures of these complexes reveal that they are isostructural and possess two copper centres that are bridged to each other by two isobidentate phosphonate ligands generating an eight-membered Cu2O2P2 ring. Magnetic studies on 2 reveal anti-ferromagnetic behaviour at low temperatures. Dinuclear complexes 1-3 were found to be excellent nucleases and can convert supercoiled pBR322 DNA form I into nick form II in only 30 min without the need for any external oxidant through a hydrolytic pathway. Wiley-VCH Verlag GmbH and Co. KGaA, 69451 Weinheim, Germany, 2009).

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Tetrahydropyran – Wikipedia,
Tetrahydropyran – an overview | ScienceDirect Topics

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499-40-1, Name is (2R,3S,4R,5R)-2,3,4,5-Tetrahydroxy-6-(((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl)oxy)hexanal, molecular formula is C12H22O11, belongs to Tetrahydropyrans compound, is a common compound. In a patnet, once mentioned the new application about 499-40-1, COA of Formula: C12H22O11

A bio-relevant supramolecular Co(ii)-complex for selective fluorescence sensing of muM range inorganic As(iii) in aqueous medium and its intracellular tracking in bacterial systems

A novel Co(ii)-complex {i.e. [Co(n-BuM)(DPA)(H2O)2]¡¤H2O} [n-BuMH2 = n-butylmalonic acid and DPA = 2,2?-dipyridylamine] was synthesized. The supramolecular feature, i.e. a metal coordinated and free guest water mediated hydrogen-bonding interaction assisted supramolecular pipi assembly, has been observed in the crystal structure of the Co(ii)-complex in the solid state. The role of different water molecules (metal coordinated and free guest water molecules) had also been scrutinized via theoretical studies. The fluorescent nature of the aqueous solution of the Co(ii)-complex has been utilized for selective muM range toxic inorganic As(iii)-sensing in aqueous medium. The Co(ii)-probe is very specific towards toxic As(OH)3 even in the presence of several ions and other arsenic sources like inorganic As(v)-oxoanions and organic arsenic species like cacodylic acid. The bio-relevant nature of the fluorescent probe of the Co(ii)-complex has also been examined. The luminous Co(ii)-probe has been employed for the intracellular tracking of As(iii) in bacterial systems including As(iii)-resistant bacteria Bacillus aryabhattai and As(iii) non-resistant bacteria Bacillus subtilis.

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Tetrahydropyran – Wikipedia,
Tetrahydropyran – an overview | ScienceDirect Topics

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499-40-1, Name is (2R,3S,4R,5R)-2,3,4,5-Tetrahydroxy-6-(((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl)oxy)hexanal, molecular formula is C12H22O11, belongs to Tetrahydropyrans compound, is a common compound. In a patnet, once mentioned the new application about 499-40-1, Product Details of 499-40-1

Synthesis, characterization and reactivity of arene ruthenium compounds based on 2,2?-dipyridylamine and di-2-pyridylbenzylamine and their applications in catalytic hydrogen transfer of ketones

The synthesis and characterization of cationic arene ruthenium compounds [(eta6-p-iPrC6H4Me) RuCl(kappa2-dpa)]BF4 (1), [(eta6-C 6H6)RuCl(kappa2-dpa)]BF4 (2), [(eta6-p-iPrC6H4Me)- RuCl(kappa2-dpb)]BF4 (3), [(eta6-p- iPrC6H4Me)RuCl(kappa2-dpb)]PF 6.CH3OH (4) and [(eta6-C6H 6)-RuCl(kappa2-dpb)]PF6 (5) (arene = C 6H6 or p-iPrC6H4Me; dpa = 2,2?-dipyridylamine and dpb = di-2-pyridylbenzylamine) have been described. Reactions of the representative compounds 1 and 3 with NaN 3, NaCN, and NH4SCN afforded substitution products [(eta6-p-iPrC6H4Me)- Ru(kappa2-dpa)(N3)]BF4 (6), [(eta6-p-iPrC6H4Me) Ru(kappa2-dpa)(CN)]BF4 (7), [(eta6-p- iPrC6H4Me)-Ru(kappa2-dpa)(NCS)] BF4 (8), [(eta6-p-iPrC6H 4Me)Ru(kappa2-dpb)(N3)]BF4 (9), [(eta6-p-iPrC6H4Me)- Ru(kappa2-dpb)(CN)]BF4 (10) and [(eta6-p- iPrC6H4Me)Ru(kappa2-dpb)(NCS)] BF4 (11). The compounds under investigation have been characterized by elemental analyses, spectroscopic and electrochemical studies. Molecular structures of 1, 3, 4 and 5 have been determined crystallographically. The compounds 1-3 and 5 exhibited moderate catalytic activity in the reduction of ketones into corresponding alcohol in absence of a base.

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Tetrahydropyran – Wikipedia,
Tetrahydropyran – an overview | ScienceDirect Topics

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Sometimes chemists are able to propose two or more mechanisms that are consistent with the available data.Formula: C12H22O11, If a proposed mechanism predicts the wrong experimental rate law, however, the mechanism must be incorrect.Welcome to check out more blogs about 499-40-1, in my other articles.

A catalyst don’t appear in the overall stoichiometry of the reaction it catalyzes, but it must appear in at least one of the elementary reactions in the mechanism for the catalyzed reaction. 499-40-1, Name is (2R,3S,4R,5R)-2,3,4,5-Tetrahydroxy-6-(((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl)oxy)hexanal, molecular formula is C12H22O11. In a Article£¬once mentioned of 499-40-1, Formula: C12H22O11

catena-poly[[(di-2-pyridyl-N-amine)-(propionato-O,O?)copper(II)]-mu -nitrato-O:O?]

The title compound, [Cu(NO3)(C3H5O2)(C 10H9N3)], contains infinite chains of a six-coordinate CuN2O2O2? chromophore. The molecular chromophore has a distorted octahedral structure, with symmetrically bonding di-2-pyridylamine (dpyam) and bidentate propionate groups defining an equatorial O2N2 plane, and axial O atoms of bridging ‘semi-coordinate’ nitrate groups completing the sixfold coordination.

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Reference£º
Tetrahydropyran – Wikipedia,
Tetrahydropyran – an overview | ScienceDirect Topics

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Cu(NN)2Cl2 and Cu(NNN)Cl2 and HgCl 2 building blocks in the synthesis of coordination compoundsX-ray studies and magnetic properties

A series of complexes containing Cu(NN)2Cl2 (NN=bis(pyrazol-1-yl)methane (bpzm), bis(3,5dimethylpyrazol-1-yl)methane (bdmpzm), 2,2-dipyridylamine (dpa), 5,6-diphenyl-3-(2-pyridyl)-1,2,4-trazine (dppt) and 2,2?-bipyridine (bipy)), Cu(NNN)Cl2 (NNN=2,2?:6?,2?-terpyridine (terpy)) and HgCl2 building blocks have been synthesized and structurally characterized. Increase in structural dimensionality is observed for [Cu(bpzm)2][HgCl 4], [Cu(dpa)2][HgCl3]2 and [Cu(terpy)(mu-Cl)HgCl3] compounds. No coordination polymers have formed in the case of bis(3,5dimethylpyrazol-1-yl)methane, 5,6-diphenyl-3-(2- pyridyl)-1,2,4-trazine and 2,2?-bipyridine. The [Cu(bpzm) 2][HgCl4] and [Cu(terpy)(mu-Cl)HgCl3] complexes have been studied by magnetic measurements.

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Reference£º
Tetrahydropyran – Wikipedia,
Tetrahydropyran – an overview | ScienceDirect Topics