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The invention discloses a nitrogen-containing heterocyclic derivatives and their application in the retinal disease, nitrogen-containing heterocyclic derivatives is the formula Wherein R1 , R2 , R3 , R4 Independently selected from – H or – F. In the 5 mug/mL under the same concentration, the implementation of the example two, implementation […] HRCEC […] and implementation of growth inhibition rate of the superior to the monoclonal antibody medicine Avastin. To the intravitreal injection after administration, the compounds of the invention can reduce the pathological neovascularization, illustrate the invention nitrogen-containing heterocyclic […] I or the salts thereof can be used for the treatment of retinal angiogenesis related diseases in-depth research and development, the diseases such as retinal vein occlusion, shelter for diabetic retinopathy, retinal new blood vessel membrane, neovascular glaucoma, premature retinopathy, such as proliferative vitreoretinopathy. (by machine translation)

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Reference:
Tetrahydropyran – Wikipedia,
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The invention relates to new compounds that are suitable as contrast media especially for infarction and necrosis imaging, process for their production and pharmaceutical agents that contain these compounds.

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Three new substituted tetraphenylene crown ethers have been made. Bis(5- carbomethoxy-1,3-phenylene)-bis(p-phenylene)-(3x + 6)-crown-x, where x = 12, 16, and 20 (11b-11d) were synthesized via [1 + 1] cyclization of methyl 3,5- bis[omega-chloro(oligoethyleneoxy)]benzoates (13b-3d) with methyl 3,5-bis[omega- (p-hydroxyphenoxy)(oligoethyleneoxy)]benzoates (16b-6d) using K2CO3 as base and tetrabutylammonium iodide as a phase transfer agent in dimethylformamide (DMF). The corresponding 30-membered (x = 8) macrocycle 11a could not be made by this approach; only the elimination product, 3,5-bis(vinyloxy)benzoic acid (19), was isolated. 16a-16d were made via alkylation of p-benzyloxyphenol (14) with 13a-13d, respectively, followed by hydrogenolysis with Pd/C as catalyst. No complexation of these macrocycles with dibenzylammonium ions was detected by NMR spectroscopy, but weak complexation of 11d with a paraquat derivative was observed.

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Reference:
Tetrahydropyran – Wikipedia,
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An efficient, two-step synthetic method for the addition of ethyleneoxy units to diols is reported.Reaction of HOROH with Cl(CH2CH2O)nTHP and 50percent aqueous NaOH in the presence of a phase-transfer catalyst gives THP(OCH2CH2)nORO(CH2CH2O)nTHP from which the protecting groups are readily removed to provide H(OCH2CH2)nORO(CH2CH2O)n in good-to-excellent yields.The influence of reactant diol structure upon yield has been determined.

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We demonstrate that MWCNTs can be dispersed in common organic solvents as single tubes using a single hexabenzocoronene (HBC) unit at the end of a poly(methyl methacrylate) (PMMA) chain. The concentration of the HBC-based additive needed to disperse MWCNTs is substantially lower than the concentration needed for existing additives.

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In homogeneous catalysis, the catalyst is in the same phase as the reactant. The number of collisions between reactants and catalyst is at a maximum. Electric Literature of 5631-96-9, Electric Literature of 5631-96-9, C7H13ClO2. A document type is Article, introducing its new discovery.

The synthesis and spectroscopic investigation of the new noncyclic neutral ligands 12-20 of the glycol ether type (podands) carrying terminal electron-donor- and -acceptor groups are described.The podands show intramolecular charge transfer interactions which can be influenced selectively by complexed cations.The ligands 13 and 20 cause significant increases of extinction and bathochromic shifts of the charge transfer bands in the UV/Vis spectra on addition of alkali perchlorates, whereas the shorter ligands 14 and 18 show a decrease of extinction and hypsochromic shifts under similar conditions.Some of the noncyclic chromoionophores discern considerably and visually perceivably between Na+ and K+ or Li+ and Na+, respectively, in acetonitrile.The cation selective alterations in the electron spectra are discussed in view of steric effects considering some complex stability constants determined by photometric titrations.

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The invention relates to a procedure for preparing quetiapine by reaction between a compound of formula (II) and a compound of formula (III), in which X means a leaving group and P a protective group of alcohols resistant to alkaline conditions, in the presence of a base, followed by a step of deprotection and, optionally, obtaining a pharmaceutically acceptable salt thereof. Said procedure permits the obtaining of quetiapine with a high degree of purity under soft temperature conditions, with short reaction times and avoiding the use of toxic solvents.

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Reference:
Tetrahydropyran – Wikipedia,
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Symmetrical nitrogen containing ring structures with two or four glucose units were easily obtained from accessible monosaccharide building units. Various tetherings via 4,4′- and 6,6′-positions lead to a variety of precursors which were transformed successively employing different bridging units by Richman-Atkins cyclisation to result in defined glycophane coronands.

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The cis-2-alkyl-3-oxy-tetrahydropyran unit as a novel structure for the design and synthesis of a new type of ionophores with C2-symmetry is reported. The synthesis of seven different macrolides and a crown ether and their cation complexation properties were investigated. The X-ray crystal structure of some of the receptors provides valuable information on the preferred conformation of tetrahydropyrans in the solid state that can be related to the cation complexation properties in solution. The kinetic template effect has been proved to be a useful tool to improve the yield and selectivity in the synthesis of macrodiolide 3.

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This invention provides heterocyclic compounds that bind to E3 Ubiquitin Ligase (typically through cereblon) (“Degrons”), which can be used as is or linked to a Targeting Ligand for a selected Target Protein for therapeutic purposes and methods of use and compositions thereof as well as methods for their preparation.

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Reference:
Tetrahydropyran – Wikipedia,
Tetrahydropyran – an overview | ScienceDirect Topics